ISO 4097:2014 pdf free
ISO 4097:2014 pdf free.Rubber, ethylene-propylene-diene (EPDM)一Evaluation procedure
ISO 4097 specifies the following:
– physical and chemical tests on raw rubbers;
– standard materials, standard test formulations, equipment, and processing methods for evaluating the vulcanization characteristics of ethylene-propylene-diene rubbers (EPDM), including oil-extended types.
2 Normative references
The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 37, Rubber, vulcanized or thermoplastic一Determination of tensile stress-strain properties
ISO 247, Rubber一Determination of ash
ISO 248-1, Rubber, raw一Determination of volatile-matter content一Part 1: Hot-mill method and oven method
ISO 248-2, Rubber, raw一Determination of volatile-matter content一Part 2: Thermogravimetric methods using an automatic analyser with an infrared drying unit
ISO 289-1, Rubber; unvulcanised一Determinations using a shearing-disc viscometer- Part 1: Determination of Mooney viscosity
ISO 1795, Rubber, raw natural and raw synthetic一Sampling and further preparative procedures
ISO 2393, Rubber test mixes一Preparation, mixing and vulcanization一Equipment and procedures
ISO 3417, Rubber一Measurement of vulcanization characteristics with the oscillating disc curemeter
ISO 6502, Rubber一Guide to the use of curemeters
ISO 23529, Rubber一General procedures for preparing and conditioning test pieces for physical test methods
Determine the Mooney viscosity in accordance with IS0 289-1, on a test portion prepared as indicated in 3.2 (without massing).
If massing is necessary, maintain the mill roll surface temperature at 50 °C±5 °C (for rubbers with a low Mooney viscosity, a temperature of 35 °C±5 °C can be used). Massing, if used, shall be mentioned in the test report.
Record the result as ML(1+4) at 125 °C unless another test temperature (100 °C or 150 °C) and/or test time (1+8) min has been agreed by the interested parties.
The standard test formulations are given in Table 1, in which:
a) formulation 1 is applicable to non-oil-extended EPDMs with a nominal ethylene content not higher than 67 % by mass;
b) formulation 2 is applicable to non-oil-extended EPDMs with a nominal ethylene content equal to or higher than 67 % by mass;
c) formulation 3 is applicable to non-oil-extended low Mooney viscosity EPDMs;
d) formulation 4 is applicable to oil-extended EPDMS containing 50 or less parts by mass of oil per 100 parts of rubber;
e) formulation 5 is applicable to oil-extended EPDMs containing more than 50 but less than 80 parts by mass of oil per 100 parts of rubber;
f) formulation 6 is applicable to oil-extended EPDMs containing 80 or more parts by mass of oil per 100 parts of rubber.ISO 4097 pdf download.