ISO 247-2:2018 pdf free
ISO 247-2:2018 pdf free.Rubber- Determination of ash – Thermogravimetric analysis (TGA)
This document specifies two methods for the determination of ash from raw rubbers, compounded rubbers and vulcanizates using a thermogravimetric analyser (TGA).
The methods are applicable to raw, compounded or vulcanized rubbers of the M, 0, R and U families described in ISO 1629:
一Method A is applicable for the determination of the ash from raw rubbers.
一 Method B is applicable for the determination of the ash from compounded or vulcanized rubbers.
The methods are not applicable for the determination of the ash from raw rubbers, compounded or vulcanized rubbers containing chlorine, bromine or iodine.
This document does not cover the interpretation of the ash results from the inorganic chemical contents of compounded or vulcanized rubbers.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content constitutes requirements of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 248-1, Rubber, raw一Determination of volatile-matter content一Part 1: Hot-mill method and oven method
ISO 1795, Rubber, raw natural and raw synthetic一Sampling and further preparative procedures
3 Terms and definitions
No terms and definitions are listed in this document.
ISO and IEC maintain terminological databases for use in standardization at the following addresses:
一IEC Electropedia: available at hts://www.electropedia.org/
一ISO Online browsing platform: available at https://www.iso.org/obp
4 Principle
A weighed test portion is heated in an atmosphere of nitrogen. After complete decomposition of the polymer, the atmosphere is switched from nitrogen to oxygen or air and the test portion is further heated untill all the carbonaceous matter has been burnt off and a constant mass is reached. The mass of the residue represents the ash.
For raw natural rubber, test samples shall be cut from the homogenized piece prepared in accordance with ISo 1795. For raw synthetic rubber, test samples shall be cut from the dried rubber obtained after carrying out the determination of volatile-matter content in accordance with the hot-mill
method of ISO 248-1.
Take a test portion of about 2 g to 5 g from the homogenized sample and cut into pieces by hand.ISO 247-2 pdf download.
